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            石油產品類水分測定方法分析

            文章出處:未知人氣: 169 發布時間:2018-11-23 16:09
                   石油產品測試水分主要有兩個目的,一是計量油品數量,油品檢尺后減去水分,可計算出整個容器油品的實際量;二是測出水分含量,確定有效的脫水方法,防止造成危害。

                   石油產品含水可造成很多危害:1、石油產品中水分蒸發時會吸收熱量,使油品的發熱量降低;2、在低溫情況下,發動機燃料中的水分會結冰,堵塞發動機燃料導管和濾清器,妨礙燃料系統正常供油;3、輕質石油產品中的水分會使燃燒過程惡化,并能將溶解于水中的鹽帶入氣缸內,生產積碳,增加氣缸的磨損;4、石油產品中含有水分時,會加速油品的氧化和生膠;5、潤滑油中含水時,能促使潤滑油乳化,破壞潤滑油油膜和潤滑性能。

                   石油產品的水分測定方法主要有:目測法、蒸餾法和卡爾費休法。目測法是靠人眼去觀察的,誤差很大,有很大的不準確性,只能做出一個大概的判斷,局限性比較大。蒸餾法常用的蒸餾裝置,用標準磨口儀器裝配,由圓底燒瓶、蒸餾頭、溫度計、冷凝管、接收管和接收瓶組成。當用普通玻璃儀器裝配蒸餾裝置時,通常使用帶支管的蒸餾燒瓶,各玻璃儀器間用膠塞連接。全套組裝比較麻煩,且具體測試時要根據測試量選擇合適的蒸餾瓶,操作步驟繁瑣且要求高,不適用于快速檢測油品水分。

                   目前用的最多的是卡爾費休法水分儀,以AKD-A5智能卡爾費休微量水分儀為例,采用卡爾-費休庫侖法,是世界公認的測試水含量的方法。儀器采用了功能強大的新一代處理器,雙CPU設計,大大提高了運算效率。雙電源通道的設計使電解電極和測量電極分離,儀器能夠自動去除各類干擾,使測試結果精密度大大提高,可達到0.0001%(1ppm)。內置多種運算公式,滿足不同樣品的測試需求,可存儲500條實驗數據,同時配置打印機,直接打印出試驗數據。卡爾費休微量水分儀具有測量精度高、重復性好、測試成本低等優點,被廣泛應用于石油、化工、醫藥、電力、科研和教育等部門,可用于測量各種液體、固體和氣體中的微量水分。

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